Investigation of mechanical properties of polymer impregnated concrete containing polypropylene fiber by taguchi and anova methods

  • Harun Tanyildizi Department of Civil Engineering, Technology Faculty, Firat University, TR-23119, Elazig (Turkey)
Keywords: polypropylene fiber, mechanical properties, taguchi, anova analysis, polymer impregnated concrete


The mechanical properties of polymer impregnated concrete containing polypropylene fiber were statistically and experimentally examined in this study. Taguchi L9 (33) was used in this study. The variables used for experiments were selected as the polypropylene fiber ratio (0%, 1% and 2%), cement dosage (300, 350 and 400 kg/m3) and curing time (7, 14 and 28 days). After the specimens were cured at the specified curing times, they were dried at 105 ±5 °C. Then, the monomer was impregnated to the specimens for 24 hours under atmospheric conditions. The samples for the polymerization of monomer was kept within the drying oven at 60 °C for 6 hours. The compressive strength and ultrasonic pulse velocity tests of specimens, in which polymerization was applied, was conducted. Furthermore, the dynamic modulus of elasticity of samples was calculated using the ultrasonic pulse velocity. The Taguchi analysis found that the best values for the ultrasonic pulse velocity, dynamic modulus of elasticity and compressive strength were 28 days for curing, 1% for the polypropylene fiber percentage and 400 kg/m3 for the cement dosage. The Anova analysis found that the polypropylene fiber percentage had the biggest effect on the mechanical properties of polymer impregnated concrete containing polypropylene fiber.

Author Biography

Harun Tanyildizi, Department of Civil Engineering, Technology Faculty, Firat University, TR-23119, Elazig (Turkey)

Department of Civil Engineering, Technology Faculty, Firat University

Elazig, 23119 (Turkey)


Akça, K. I. R., Çakir, Ö., & Ipek, M. (2015). Properties of polypropylene fiber reinforced concrete using recycled aggregates. Construction and Building Materials, 98, 620–630.

Al-Rousan, R. Z., Haddad, R. H., & Swesi, A. O. (2015). Repair of shear-deficient normal weight concrete beams damaged by thermal shock using advanced composite materials. Composites Part B: Engineering, 70, 20–34.

Alfahdawi, I. H., Osman, S. A., Hamid, R., & Al-Hadithi, A. I. (2018). Modulus of elasticity and ultrasonic pulse velocity of concrete containing polyethylene terephthalate (pet) waste heated to high temperature. Journal of Engineering Science and Technology, 13(11), 3577–3592.

ASTM C597. (2016). Standard Test Method for Pulse Velocity Through Concrete. American Society for Testing and Materials, West Conshohocken, PA, USA.

Atis, C. D., Tanyildizi, H., & Karahan, O. (2009). Statistical analysis for strength properties of polypropylene-fibre- reinforced fly ash concrete. Magazine of Concrete Research, 61(7), 557–566.

Auskern, A., & Horn, W. (1971). Some properties of polymer impregnated cements and concretes. Composites, 2(4), 257.

Awal, A. S. M. A., & Shehu, I. A. (2015). Performance evaluation of concrete containing high volume palm oil fuel ash exposed to elevated temperature. Construction and Building Materials, 76, 214–220.

Bal, H. (1999). Investigation of the usability of some polymers in mortars. MSc thesis, Firat Univ., Elazig.

Behfarnia, K., & Behravan, A. (2014). Application of high performance polypropylene fibers in concrete lining of water tunnels. Materials and Design, 55, 274–279.

Behfarnia, K., & Farshadfar, O. (2013). The effects of pozzolanic binders and polypropylene fibers on durability of SCC to magnesium sulfate attack. Construction and Building Materials, 38, 64–71.

Bhutta, M. A. R., Maruya, T., & Tsuruta, K. (2013). Use of polymer-impregnated concrete permanent form in marine environment: 10-year outdoor exposure in Saudi Arabia. Construction and Building Materials, 43, 50–57.

Bogas, J. A., Gomes, M. G., & Gomes, A. (2013). Compressive strength evaluation of structural lightweight concrete by non-destructive ultrasonic pulse velocity method. Ultrasonics, 53(5), 962–972.

Carstens, P. A. B., Marais, S. A., & Thompson, C. J. (2000). Improved and novel surface fluorinated products. Journal of Fluorine Chemistry, 104(1), 97–107.

Chandra, S., & Ohama, Y. (1994). Polymers in concrete. United States: CRC press. Available on:

Chandrappa, A. K., & Biligiri, K. P. (2016). Influence of mix parameters on pore properties and modulus of pervious concrete: an application of ultrasonic pulse velocity. Materials and Structures/Materiaux et Constructions, 49(12), 5255–5271.

Chen, C. H., Huang, R., Wu, J. K., & Chen, C. H. (2006). Influence of soaking and polymerization conditions on the properties of polymer concrete. Construction and Building Materials, 20(9), 706–712.

Chmielewska, B. (2008). Adhesion Strength and Other Mechanical Properties of SBR Modified Concrete. International Journal of Concrete Structures and Materials, 2(1), 3–8.

Czigány, T. (2006). Special manufacturing and characteristics of basalt fiber reinforced hybrid polypropylene composites: Mechanical properties and acoustic emission study. Composites Science and Technology, 66(16), 3210–3220.

Davim, J. P. (2001). A note on the determination of optimal cutting conditions for surface finish obtained in turning using design of experiments. Journal of Materials Processing Technology, 116(2–3), 305–308.

Deák, T., Czigány, T., Tamás, P., & Németh, C. (2010). Enhancement of interfacial properties of basalt fiber reinforced nylon 6 matrix composites with silane coupling agents. Express Polymer Letters, 4(10), 590–598.

Ezziane, M., Kadri, T., Molez, L., Jauberthie, R., & Belhacen, A. (2015). High temperature behaviour of polypropylene fibres reinforced mortars. Fire Safety Journal, 71, 324–331.

Ghaffari Moghaddam, F., Akbarpour, A., & Firouzi, A. (2021). Dynamic modulus of elasticity and compressive strength evaluations of modified reactive powder concrete (MRPC) by non-destructive ultrasonic pulse velocity method. Journal of Asian Architecture and Building Engineering, 2020, 1-10.

Grdic, Z. J., Curcic, G. A. T., Ristic, N. S., & Despotovic, I. M. (2012). Abrasion resistance of concrete micro-reinforced with polypropylene fibers. Construction and Building Materials, 27(1), 305–312.

Grzybowski, M., & Shah, S. P. (1990). Shrinkage cracking of fiber reinforced concrete, 87(2), 138–148. Available on:

Güneyisi, E., Gesoʇlu, M., Booya, E., & Mermerdaş, K. (2015). Strength and permeability properties of self-compacting concrete with cold bonded fly ash lightweight aggregate. Construction and Building Materials, 74, 17–24.

Heidarnezhad, F., Jafari, K., & Ozbakkaloglu, T. (2020). Effect of polymer content and temperature on mechanical properties of lightweight polymer concrete. Construction and Building Materials, 260, 119853.

Kadela, M., Kukiełka, A., & Małek, M. (2020). Characteristics of Lightweight Concrete Based on a Synthetic Polymer Foaming Agent. Materials, 13(21), 4979.

Karahan, O., Tanyildizi, H., & Atis, C. D. (2008). An artificial neural network approach for prediction of long-term strength properties of steel fiber reinforced concrete containing fly ash. Journal of Zhejiang University: Science A, 9(11), 1514–1523.

Kewalramani, M. A., & Gupta, R. (2006). Concrete compressive strength prediction using ultrasonic pulse velocity through artificial neural networks. Automation in Construction, 15(3), 374–379.

Li, J. (2009). The research on the interfacial compatibility of polypropylene composite filled with surface treated carbon fiber. Applied Surface Science, 255(20), 8682–8684.

Lin, Y., Hsiao, C., Yang, H., & Lin, Y. F. (2011). The effect of post-fire-curing on strengthvelocity relationship for nondestructive assessment of fire-damaged concrete strength. Fire Safety Journal, 46(4), 178–185.

Liu, G., Cheng, W., & Chen, L. (2017). Investigating and optimizing the mix proportion of pumping wet-mix shotcrete with polypropylene fiber. Construction and Building Materials, 150, 14–23.

López-Buendía, A. M., Romero-Sánchez, M. D., Climent, V., & Guillem, C. (2013). Surface treated polypropylene (PP) fibres for reinforced concrete. Cement and Concrete Research, 54, 29–35.

Małek, M., Jackowski, M., Łasica, W., & Kadela, M. (2020). Characteristics of recycled polypropylene fibers as an addition to concrete fabrication based on portland cement. Materials, 13(8), 1827.

Matkó, S., Anna, P., Marosi, G., Szép, A., Keszei, S., Czigány, T., & Pölöskei, K. (2003). Use of Reactive Surfactants in Basalt Fiber Reinforced Polypropylene Composites. In Macromolecular Symposia (Vol. 202, pp. 255–268). Weinheim: WILEY‐VCH Verlag.

Monteiro, P. J. M., & Mehta, P. K. (2006). Concrete: Microstructure, Properties and Materials | Request PDF (Mc Graw Hill). Available on:

Monteny, J., De Belie, N., Yincke, E., Beeldens, A., & Taerwe, L. (2001). Simulation of corrosion in sewer systems by laboratory testing. In Proceedings - fib-Symposium on Concrete and Environment 2001 (pp. 91–92). Deutscher Beton und Bautechnik Verein E.V (German Society for Concrete and Construction Technology).

Moreira, P. M., Aguiar, J. B., & Camões, A. (2006). Systems for superficial protection of concretes. In ISPIC 2006 International Symposium on Polymers in Concrete. Guimarães. Available on:

Ogawa H., Kano K., Mimura T., Nagai K., Shirai A., O. Y. (2007). Durability Performance of Barrier Penetrants on Concrete Surfaces. In 12th International Congress on Polymers in Concrete (pp. 373–382). Chuncheon- Korea. Available on:

Phadke, M. (1995). Quality Engineering Using Robust Design. Prentice Hall International.

Pişkin, A. (2010). Usability of Glass Powder in Polymer Concrete. Sakarya university.

Prasad, V. D., Prakash, E. L., Abishek, M., Dev, K. U., & Kiran, C. S. (2018). Study on concrete containing Waste Foundry Sand, Fly Ash and Polypropylene fibre using Taguchi Method. Materials Today: Proceedings, 5(11), 23964-23973.

Puy, G. W. D., & Dikeou, J. T. (1974). Polymer in concrete. American Concrete Institute. Available on:

Ross, P. J. (1996). Taguchi Techniques for Quality Engineering: Loss Function, Orthogonal Experiments, Parameter and Tolerance Design. Available on:

Shariq, M., Prasad, J., & Masood, A. (2013). Studies in ultrasonic pulse velocity of concrete containing GGBFS. Construction and Building Materials, 40, 944–950.

Shıraı A., Kano K., Nagai K., Ide K., Ogawa H., O. Y. (2007). Basic Properties of Barrier Penetrants as Polymeric Impregnants For Concrete Surfaces. In 12th International Congress on Polymers in Concrete, (pp. 607–615). Chuncheon-Korea. Available on:

Sidney, R., & Young, J. F. (1981). Concrete. Prentice Hall. Englewood Cliffs. Available on:

Sobczak, L., Brüggemann, O., & Putz, R. F. (2013). Polyolefin composites with natural fibers and wood‐modification of the fiber/filler–matrix interaction. Journal of Applied Polymer Science, 127(1), 1-17.

Srubar, W. V. (2015). Stochastic service-life modeling of chloride-induced corrosion in recycled-aggregate concrete. Cement and Concrete Composites, 55, 103–111.

Swamy, R. N., & Bouikni, A. (1990). Some engineering properties of slag concrete as influenced by mix proportioning and curing. ACI Materials Journal, 87(3), 210–220.

Tanaka, T., Tsuruta, K., & Naitou, T. Development and application of polymer impregnated concrete. In Proc of the first fib congress, Osaka, concrete structures in the 21st century 6 (pp. 347–354), Osaka, Japan, October, 2002.

Tanyildizi, H. (2014). Post-fire behavior of structural lightweight concrete designed by Taguchi method. Construction and Building Materials, 68, 565–571.

Tanyildizi, H. (2018a). Long-term microstructure and mechanical properties of polymer-phosphazene concrete exposed to freeze-thaw. Construction and Building Materials, 187, 1121–1129.

Tanyildizi, H. (2018b). Long-term performance of the healed mortar with polymer containing phosphazene after exposed to sulfate attack. Construction and Building Materials, 167, 473–481.

TANYILDIZI, H. (2020). Investigation of carbonation performance of polymer-phosphazene concrete using Taguchi optimization method. Construction and Building Materials, 273, 121673.

Tanyildizi, H., & Asilturk, E. (2018a). High temperature resistance of polymer-phosphazene concrete for 365 days. Construction and Building Materials, 174, 741–748.

Tanyildizi, H., & Asilturk, E. (2018b). Performance of Phosphazene-Containing Polymer-Strengthened Concrete after Exposure to High Temperatures. Journal of Materials in Civil Engineering, 30(12), 04018329.

Tanyildizi, H., Coşkun, A., & Somunkiran, I. (2008). An experimental investigation of bond and compressive strength of concrete with mineral admixtures at high temperatures. Arabian Journal for Science and Engineering, 33(2B), 443–449. Available on:

Tanyildizi, H., & Şahin, M. (2017). Taguchi optimization approach for the polypropylene fiber reinforced concrete strengthening with polymer after high temperature. Structural and Multidisciplinary Optimization, 55(2), 529–534.

Tenza-Abril, A. J., Benavente, D., Pla, C., Baeza-Brotons, F., Valdes-Abellan, J., & Solak, A. M. (2020). Statistical and experimental study for determining the influence of the segregation phenomenon on physical and mechanical properties of lightweight concrete. Construction and Building Materials, 238, 117642.

Tosun, G., & Tosun, N. (2012). Analysis of process parameters for porosity in porous NiTi implants. Materials and Manufacturing Processes, 27(11), 1184–1188.

TS EN 12390-3. (2019). Testing Hardened Concrete Part 3: Compressive Strength of Test Specimens. Turkey. Available on:

Unterweger, C., Brüggemann, O., & Fürst, C. (2014a). Effects of different fibers on the properties of short-fiber-reinforced polypropylene composites. Composites Science and Technology, 103, 49-55.

Unterweger, C., Brüggemann, O., & Fürst, C. (2014b). Synthetic fibers and thermoplastic short-fiber-reinforced polymers: Properties and characterization. Polymer Composites, 35(2), 227–236.

Uysal, M., Akyuncu, V., Tanyildizi, H., Sumer, M., & Yildirim, H. (2019). Optimization of durability properties of concrete containing fly ash using Taguchi’s approach and Anova analysis. Revista de La Construccion, 17(3), 364–382.

Whiting, D., & Kline, D. E. (1976). Theoretical predictions of the elastic moduli of polymer-impregnated hardened cement paste and mortars. Journal of Applied Polymer Science, 20(12), 3353–3363.

Yalçın, F. (1998). Studies of some mechanical properties of polymer impregnated concrete. MSc thesis, Cumhuriyet Univ., Sivas.

Yang, Z., Shi, X., Creighton, A. T., & Peterson, M. M. (2009). Effect of styrene-butadiene rubber latex on the chloride permeability and microstructure of Portland cement mortar. Construction and Building Materials, 23(6), 2283–2290.

Yermak, N., Pliya, P., Beaucour, A. L., Simon, A., & Noumowé, A. (2017). Influence of steel and/or polypropylene fibres on the behaviour of concrete at high temperature: Spalling, transfer and mechanical properties. Construction and Building Materials, 132, 240–250.

Yılmaz, B., Dinç, A., Şengül, C., Akaya, Y., & Taşdemir, M. (2007). Effects of cement/powder ratio on workability and mechanical behaviour of SCFRCs. In International conferance on ACBM (p. 11). Lahore: ACI. Available on:

Zoalfakar, S. H., Elsissy, M. A. R., & Shaheen, Y. B. (2020). Multi-Response Optimization of Post-Fire Residual Properties of High Performance Concrete. Bulletin of the Faculty of Engineering. Mansoura University, 40(1), 83-97.